advanced
Journal Information
Journal Information
   Description
   Editorial Board
   Guide for Authors
   Ordering

Contents Services
Contents Services
   Regular Issues
   Special Issues
   Authors Index

Links
Links
   FEI STU Bratislava
   SAS Bratislava

   Feedback

[5, 2010] 

Journal of Electrical Engineering, Vol 61, 5 (2010) 299-301

PROPERTIES OF FeCo NANOPOWDER PREPARED BY CHEMICAL SYNTHESIS

Karel Zábranský – Oldřich Schneeweiss

   Chemical synthesis of binary Fe-Co oxalate was used for preparation of Fe-Co nanoparticles. X-ray difftaction spectra recorded during temperature treatment in reduction atmosphere show two main stages of transformation: amorphization of the oxalate mixture and formation of Fe-Co nanoparticles. After X-ray diffraction high temperature treatment the nanoparticles with 50 nm mean crystallite were found. Comparison of magnetic properties during and after different type of temperature treatment shows that coercivity and saturation magnetic polarization are sensitive in dependence on sample condition, length of treatment and temperature. Analysis of Mössbauer spectra reveal several components which were ascribed different phases during temperature treatments.


[full-paper]


© 1997-2019  FEI STU Bratislava